Mixed Bed Demineralizer

 
Reduced Throughput / Poor Effluent Quality
Possible Cause Solution
NOTE: Most comments for cation and anion apply to mixed-bed demineralizers and for best performance always use mixed-bed grade resin.
Poor primary exchanger performance
  · Troubleshoot primary cation and anion exchangers
Poor separation of mixed bed in first step of regeneration
  · Check flowrates and temperature of backwash water

· Check for proper resin vs mid-collector interface location

· Insure use of mixed-bed grade resin
Interface too low because of loss of cation resin
  · Add cation resin
Interface too high because of separation and anion trapped within cation bed
  · Check flowrates and temperature of backwash water

· Correct flowrates
Interface too high because of overcharging of cation resin
  · Remove appropriate amount of cation resin
Cross contamination
  · Result of poor separation of the cation and anion resins, improper interface location due to los of overcharging of cation resin
Acid in the anion zone which causes SO4 leakage and early anion exhaustion
  · Insure adequate blocking flow
Caustic in the cation zone which causes Na leakage and early cation exhaustion
  · Insure adequate blocking flow
Insufficient displacement rinse which results in resin cross contamination and high effluent conductivity
  · Extend displacement rinse to achieve acceptable conductivity
Insufficient mixinf after regeneration step caused by insufficient air flow
  · Check and adjust air flow
Improper draindown prior to air mix
  · Check water level prior to air mix

· Adjust setting for water level
Fluidization and reseparation of the bed during refill due to excess flowrate
  · Perform a slow fill through the caustic distributor followed by a fast fill through the service inlet
Excessive Final Rinse
  · Poor resin separation (see above)

· Cross contamination (see above)
Premature silica break
· Silica precipitation due to contact with acid · Start acid injection 20 minutes after start of caustic injection